Tetranitroresorcin[4]arene: synthesis and structure of a new stereoisomer

Ngong Kodiah Beyeh; Kari Rissanen

doi:10.1016/j.tetlet.2009.10.075

Tetranitroresorcin[4]arene: synthesis and structure of a new stereoisomer

Ngong Kodiah Beyeh, Kari Rissanen

Ei julkaistu Aalto-yliopiston affiliaatiolla

University of Jyväskylä

Tutkimustuotos: Lehtiartikkeli › Article › Scientific › vertaisarvioitu

7 Sitaatiot (Scopus)

Abstrakti

The direct reaction between 2-nitroresorcinol and acetaldehyde in alkaline medium yields tetranitro-C1-resorcin[4]arene in a moderate 8.2% overall yield which was characterized by single crystal X-ray crystallography, 1H NMR spectroscopy and electrospray ionization mass spectrometry (ESI-MS). In solution and in the solid state, the product adopts a unique, thermally stable and unprecedented rcct-boat conformation.

Alkuperäiskieli	Englanti
Sivut	7369–7373
Julkaisu	Tetrahedron Letters
Vuosikerta	50
Numero	52
DOI - pysyväislinkit	https://doi.org/10.1016/j.tetlet.2009.10.075
Tila	Julkaistu - jouluk. 2009
OKM-julkaisutyyppi	A1 Alkuperäisartikkeli tieteellisessä aikakauslehdessä

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10.1016/j.tetlet.2009.10.075

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title = "Tetranitroresorcin[4]arene: synthesis and structure of a new stereoisomer",

abstract = "The direct reaction between 2-nitroresorcinol and acetaldehyde in alkaline medium yields tetranitro-C1-resorcin[4]arene in a moderate 8.2% overall yield which was characterized by single crystal X-ray crystallography, 1H NMR spectroscopy and electrospray ionization mass spectrometry (ESI-MS). In solution and in the solid state, the product adopts a unique, thermally stable and unprecedented rcct-boat conformation.",

author = "Beyeh, {Ngong Kodiah} and Kari Rissanen",

year = "2009",

month = dec,

doi = "10.1016/j.tetlet.2009.10.075",

language = "English",

volume = "50",

pages = "7369–7373",

journal = "Tetrahedron Letters",

issn = "0040-4039",

publisher = "Elsevier Ltd",

number = "52",

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TY - JOUR

T1 - Tetranitroresorcin[4]arene: synthesis and structure of a new stereoisomer

AU - Beyeh, Ngong Kodiah

AU - Rissanen, Kari

PY - 2009/12

Y1 - 2009/12

N2 - The direct reaction between 2-nitroresorcinol and acetaldehyde in alkaline medium yields tetranitro-C1-resorcin[4]arene in a moderate 8.2% overall yield which was characterized by single crystal X-ray crystallography, 1H NMR spectroscopy and electrospray ionization mass spectrometry (ESI-MS). In solution and in the solid state, the product adopts a unique, thermally stable and unprecedented rcct-boat conformation.

AB - The direct reaction between 2-nitroresorcinol and acetaldehyde in alkaline medium yields tetranitro-C1-resorcin[4]arene in a moderate 8.2% overall yield which was characterized by single crystal X-ray crystallography, 1H NMR spectroscopy and electrospray ionization mass spectrometry (ESI-MS). In solution and in the solid state, the product adopts a unique, thermally stable and unprecedented rcct-boat conformation.

U2 - 10.1016/j.tetlet.2009.10.075

DO - 10.1016/j.tetlet.2009.10.075

M3 - Article

SN - 0040-4039

VL - 50

SP - 7369

EP - 7373

JO - Tetrahedron Letters

JF - Tetrahedron Letters

IS - 52

ER -

Tetranitroresorcin[4]arene: synthesis and structure of a new stereoisomer

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