TY - JOUR
T1 - Rheological Behaviors of Waste Polyethylene Modified Asphalt Binder : Statistical Analysis of Interlaboratory Testing Results
AU - Wang, Di
AU - Baliello, Andrea
AU - Pinheiro, Gustavo dos Santas
AU - Poulikakos, Lily D.
AU - Tušar, Marjan
AU - Vasconcelos, Kamilla L.
AU - Kakar, Muhammad Rafiq
AU - Porot, Laurent
AU - Pasquini, Emiliano
AU - Giancontieri, Gaspare
AU - Riccardi, Chiara
AU - Pasetto, Marco
AU - Presti, Davide Lo
AU - Cannone Falchetto, Augusto
N1 - Funding Information:
The RILEM Technical Committee on Valorization of Waste and Secondary Materials for Roads (TC 279-WMR) and the members of Task Group 1 are gratefully acknowledged. The authors would also like to thank Nynas AB and Swiss company Innorecycling for supporting the interlaboratory activity by providing reference neat binder and PE-pellets, PE-shreds additives. The contribution of the Swiss National Science Foundation (205121_178991) project titled “Urban Mining for Low Noise Urban Roads and Optimized Design of Street Canyons” to the Swiss partners is also acknowledged.
Publisher Copyright:
© 2023 ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959.
PY - 2023/2/7
Y1 - 2023/2/7
N2 - This article investigated the effect of waste polyethylene (PE) on the modified asphalt binders’ rheological behavior from a statistical point of view. The interlaboratory testing results from the RILEM Technical Committee 279 Valorization of Waste and Secondary Materials for Roads Task Group 1 were used for this purpose. First, an unaged 70/100 penetration graded neat binder was selected as the reference material. Next, a single 5 % content of waste PE additives (PE-pellets and PE-shreds) was mixed with a 95 % neat binder to prepare two PE modified binders. Then, dynamic shear rheometer-based temperature-frequency sweep tests were performed over a wide range of temperatures and frequencies to evaluate the rheological properties of these three binders. Different rheological behaviors were observed in the isochronal plots at high temperatures. Based on a reproducibility precision requirement proposed for phase angle, 28°C was set as the transition temperature across the rheological behaviors. Next, according to the three rheological behaviors defined in a previous study by the authors, statistical analysis was introduced to identify sensitive rheological parameters and determine the thresholds. Results indicate that the phase angle measured above 28°C and 1.59 Hz can be used as a sensitive parameter to discriminate the three rheological behaviors of PE modified binders. The thresholds among different behaviors were also calculated as an example for phase angle measured at the highest common testing temperature of 70°C. Additional experimental evaluations on more types of PE modified binders, especially at intermediate and high temperatures, are recommended to better understand their influence on the rheological behavior of PE modified binders.
AB - This article investigated the effect of waste polyethylene (PE) on the modified asphalt binders’ rheological behavior from a statistical point of view. The interlaboratory testing results from the RILEM Technical Committee 279 Valorization of Waste and Secondary Materials for Roads Task Group 1 were used for this purpose. First, an unaged 70/100 penetration graded neat binder was selected as the reference material. Next, a single 5 % content of waste PE additives (PE-pellets and PE-shreds) was mixed with a 95 % neat binder to prepare two PE modified binders. Then, dynamic shear rheometer-based temperature-frequency sweep tests were performed over a wide range of temperatures and frequencies to evaluate the rheological properties of these three binders. Different rheological behaviors were observed in the isochronal plots at high temperatures. Based on a reproducibility precision requirement proposed for phase angle, 28°C was set as the transition temperature across the rheological behaviors. Next, according to the three rheological behaviors defined in a previous study by the authors, statistical analysis was introduced to identify sensitive rheological parameters and determine the thresholds. Results indicate that the phase angle measured above 28°C and 1.59 Hz can be used as a sensitive parameter to discriminate the three rheological behaviors of PE modified binders. The thresholds among different behaviors were also calculated as an example for phase angle measured at the highest common testing temperature of 70°C. Additional experimental evaluations on more types of PE modified binders, especially at intermediate and high temperatures, are recommended to better understand their influence on the rheological behavior of PE modified binders.
KW - dynamic shear rheometer
KW - G-R parameter
KW - modified binder
KW - phase angle
KW - polyethylene plastics
KW - rheological behavior
KW - statistical analysis
UR - http://www.scopus.com/inward/record.url?scp=85149005416&partnerID=8YFLogxK
U2 - 10.1520/JTE20220313
DO - 10.1520/JTE20220313
M3 - Article
AN - SCOPUS:85149005416
VL - 51
JO - Journal of Testing and Evaluation
JF - Journal of Testing and Evaluation
SN - 0090-3973
IS - 4
ER -