Trimethylsilylation of hydroxyl group with 1,1,1,3,3,3-hexamethyldisilazane (HMDS) catalyzed by tribromomelamine (TBM)

Arash Ghorbani-Choghamarani*, Mohammad Ali Zolfigol, Maryam Hajjami, Shila Jafari

*Corresponding author for this work

Research output: Contribution to journalArticleScientificpeer-review

22 Citations (Scopus)

Abstract

Tribromomelamine (TBM) can be used as a novel catalyst for the trimethylsilylation of alcohols and phenols with 1,1,1,3,3,3- hexamethyldisilazane (HMDS). A wide variety of hydroxyl groups were selectively protected in CH2Cl2/CH3CN under mild conditions.

Original languageEnglish
Pages (from-to)1208-1213
Number of pages6
JournalJOURNAL OF THE CHINESE CHEMICAL SOCIETY
Volume55
Issue number6
DOIs
Publication statusPublished - 2008
MoE publication typeA1 Journal article-refereed

Keywords

  • Alcohols
  • Hexamethyldisilazane (HMDS)
  • Tribromomelamine (TBM)
  • Trimethylsilylation

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