Round robin into best practices for the determination of indentation size effects

Research output: Contribution to journalArticleScientificpeer-review

Researchers

  • Ana Ruiz-moreno
  • Peter Hähner
  • Lukasz Kurpaska
  • Jacek Jagielski
  • Philippe Spätig
  • Michal Trebala
  • Simo Pekka Hannula
  • Susana Merino
  • Gonzalo de Diego
  • Hygreeva Namburi
  • Ondrej Libera
  • Dimitry Terentyev
  • Tymofii Khvan
  • Cornelia Heintze
  • Nigel Jennett

Research units

  • European Commission Joint Research Centre Institute
  • NCBJ National Centre for Nuclear Research
  • Paul Scherrer Institute
  • CIEMAT
  • Centrum Vyzkumu Rez
  • Belgian Nuclear Research Center
  • Helmholtz-Zentrum Dresden-Rossendorf
  • Coventry University

Abstract

The paper presents a statistical study of nanoindentation results obtained in seven European laboratories which have joined a round robin exercise to assess methods for the evaluation of indentation size effects. The study focuses on the characterization of ferritic/martensitic steels T91 and Eurofer97, envisaged as structural materials for nuclear fission and fusion applications, respectively. Depth-controlled single cycle measurements at various final indentation depths, force-controlled single cycle and force-controlled progressive multi-cycle measurements using Berkovich indenters at room temperature have been combined to calculate the indentation hardness and the elastic modulus as a function of depth applying the Oliver and Pharr method. Intra- and inter-laboratory variabilities have been evaluated. Elastic modulus corrections have been applied to the hardness data to compensate for materials related systematic errors, like pile-up behaviour, which is not accounted for by the Oliver and Pharr theory, and other sources of instrumental or methodological bias. The correction modifies the statistical hardness profiles and allows determining more reliable indentation size effects.

Details

Original languageEnglish
Article number130
JournalNanomaterials
Volume10
Issue number1
Publication statusPublished - 1 Jan 2020
MoE publication typeA1 Journal article-refereed

    Research areas

  • Elastic modulus correction, Ferritic/martensitic steel, Indentation size effect, Nano-mechanical, Nanoindentation, Pile-up, Small scale testing

Download statistics

No data available

ID: 40830210