Analysis of 1H and 13C{1H} NMR spectral parameters of diphenylchloroarsine, diphenylcyanoarsine, and 10-chloro-5,10-dihydrophenarsazine: identification of the compounds through reference to simulated spectra

M. Mesilaakso; E.-L. Tolppa; P. Nousiainen

doi:10.1366/0003702971940891

Analysis of ¹H and ¹³C{¹H} NMR spectral parameters of diphenylchloroarsine, diphenylcyanoarsine, and 10-chloro-5,10-dihydrophenarsazine: identification of the compounds through reference to simulated spectra

M. Mesilaakso^*, E.-L. Tolppa, P. Nousiainen

^*Corresponding author for this work

Not published at Aalto University

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Research output: Contribution to journal › Article › Scientific › peer-review

4 Citations (Scopus)

Abstract

The ¹H and ¹³C{¹H} nuclear magnetic resonance (NMR) spectra of diphenylchloroarsine, diphenylcyanoarsine, and 10-chloro-5,10-di- hydrophenarsazine were recorded from samples prepared in CDCl₃, CD₂Cl₂, and (CD3)2 CO. Spectra were analyzed, and detailed 1H NMR spectral parameters were determined by iterative analysis. Simulation of spectra and their use as reference spectra for identification of the compounds under different conditions are discussed.

Original language	English
Pages (from-to)	733-737
Number of pages	5
Journal	Applied Spectroscopy
Volume	51
Issue number	5
DOIs	https://doi.org/10.1366/0003702971940891
Publication status	Published - 1 May 1997
MoE publication type	A1 Journal article-refereed

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title = "Analysis of 1H and 13C{1H} NMR spectral parameters of diphenylchloroarsine, diphenylcyanoarsine, and 10-chloro-5,10-dihydrophenarsazine: identification of the compounds through reference to simulated spectra",

abstract = "The 1H and 13C{1H} nuclear magnetic resonance (NMR) spectra of diphenylchloroarsine, diphenylcyanoarsine, and 10-chloro-5,10-di- hydrophenarsazine were recorded from samples prepared in CDCl3, CD2Cl2, and (CD3)2 CO. Spectra were analyzed, and detailed 1H NMR spectral parameters were determined by iterative analysis. Simulation of spectra and their use as reference spectra for identification of the compounds under different conditions are discussed.",

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Analysis of ¹H and ¹³C{¹H} NMR spectral parameters of diphenylchloroarsine, diphenylcyanoarsine, and 10-chloro-5,10-dihydrophenarsazine: identification of the compounds through reference to simulated spectra. / Mesilaakso, M.; Tolppa, E.-L.; Nousiainen, P.
In: Applied Spectroscopy, Vol. 51, No. 5, 01.05.1997, p. 733-737.

Research output: Contribution to journal › Article › Scientific › peer-review

TY - JOUR

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